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Adaptive-optical 3D microscopy for microfluidic multiphase flows
Clemens Bilsing, Erik Nützenadel, Sebastian Burgmann, Jürgen Czarske, Lars Büttner
Published Published online: 26 August 2024 , doi: 10.37188/lam.2024.037

Measurements based on optical microscopy can be severely impaired if the access exhibits variations of the refractive index. In the case of fluctuating liquid-gas boundaries, refraction introduces dynamical aberrations that increase the measurement uncertainty. This is prevalent at multiphase flows (e. g. droplets, film flows) that occur in many technical applications as for example in coating and cleaning processes and the water management in fuel cells. In this paper, we present a novel approach based on adaptive optics for correcting the dynamical aberrations in real time and thus reducing the measurement uncertainty. The shape of the fluctuating water-air interface is sampled with a reflecting light beam (Fresnel Guide Star) and a Hartmann-Shack sensor which makes it possible to correct its influence with a deformable mirror in a closed loop. Three-dimensional flow measurements are achieved by using a double-helix point spread function. We measure the flow inside a sessile, oscillating 50-μl droplet on an opaque gas diffusion layer for fuel cells and show that the temporally varying refraction at the droplet surface causes a systematic underestimation of the flow field magnitude corresponding to the first droplet eigenmode which plays a major role in their detachment mechanism. We demonstrate that the adaptive optics correction is able to reduce this systematic error. Hence, the adaptive optics system can pave the way to a deeper understanding of water droplet formation and detachment which can help to improve the efficiency of fuels cells.

Magnetic field-assisted batch polishing method for the mass production of precision optical glass components
Yee Man Loh, Chunjin Wang, Rui Gao, Lai Ting Ho, Chi Fai Cheung
Published Published online: 26 August 2024 , doi: 10.37188/lam.2024.028

The demand for optical glass has been rapidly increasing in various industries, where an ultra-smooth surface and form accuracy are critical for the functional elements of the applications. To meet the high surface-quality requirements, a polishing process is usually adopted to finish the optical glass surface to ensure an ultra-smooth surface and eliminate sub-surface damage. However, current ultra-precision polishing processes normally polish workpieces individually, leading to a low production efficiency and high polishing costs. Current mass-finishing methods cannot be used for optical glasses. Therefore, magnetic-field-assisted batch polishing (MABP) was proposed in this study to overcome this research gap and provide an efficient and cost-effective method for industrial use. A series of polishing experiments were conducted on typical optical components under different polishing parameters to evaluate the polishing performance of MABP on optical glasses. The results demonstrated that MABP is an efficient method to simultaneously polish multiple lenses while achieving a surface roughness, indicated by the arithmetic mean height (Sa), of 0.7 nm and maintained a sub-micrometer surface form for all the workpieces. In addition, no apparent sub-surface damage was observed, indicating the significant potential for the high-quality rapid polishing of optical glasses. The proposed method is highly competitive compared to the current optical polishing methods, which has the potential to revolutionize the polishing process for small optics.

Generation of polarization-multiplexed terahertz orbital angular momentum combs via all-silicon metasurfaces
Ming-Zhe Chong, Yiwen Zhou, Zong-Kun Zhang, Jin Zhao, Yue-Yi Zhang, et al.
Published Published online: 29 July 2024 , doi: 10.37188/lam.2024.038

Electromagnetic waves carrying orbital angular momentum (OAM), namely OAM beams, are important in various fields including optics, communications, and quantum information. However, most current schemes can only generate single or several simple OAM modes. Multi-mode OAM beams are rarely seen. This paper proposes a scheme to design metasurfaces that can generate multiple polarization-multiplexed OAM modes with equal intervals and intensities (i.e., OAM combs) working in the terahertz (THz) range. As a proof of concept, we first design a metasurface to generate a pair of polarization-multiplexed OAM combs with arbitrary mode numbers. Furthermore, another metasurface is proposed to realize a pair of polarization-multiplexed OAM combs with arbitrary locations and intervals in the OAM spectrum. Experimental results agree well with full-wave simulations, verifying a great performance of OAM combs generation. Our method may provide a new solution to designing high-capacity THz devices used in multi-mode communication systems.

Dynamic 3D shape reconstruction under complex reflection and transmission conditions using multi-scale parallel single-pixel imaging
Zhoujie Wu, Haoran Wang, Feifei Chen, Xunren Li, Zhengdong Chen, et al.
Published Published online: 25 July 2024 , doi: 10.37188/lam.2024.034

Depth measurement and three-dimensional (3D) imaging under complex reflection and transmission conditions are challenging and even impossible for traditional structured light techniques, owing to the precondition of point-to-point triangulation. Despite recent progress in addressing this problem, there is still no efficient and general solution. Herein, a Fourier dual-slice projection with depth-constrained localization is presented to separate and utilize different illumination and reflection components efficiently, which can significantly decrease the number of projection patterns in each sequence from thousands to fifteen. Subsequently, multi-scale parallel single-pixel imaging (MS-PSI) is proposed based on the established and proven position-invariant theorem, which breaks the local regional assumption and enables dynamic 3D reconstruction. Our methodology successfully unveils unseen-before capabilities such as (1) accurate depth measurement under interreflection and subsurface scattering conditions, (2) dynamic measurement of the time-varying high-dynamic-range scene and through thin volumetric scattering media at a rate of 333 frames per second; (3) two-layer 3D imaging of the semitransparent surface and the object hidden behind it. The experimental results confirm that the proposed method paves the way for dynamic 3D reconstruction under complex optical field reflection and transmission conditions, benefiting imaging and sensing applications in advanced manufacturing, autonomous driving, and biomedical imaging.

Flexible orbital angular momentum mode switching in multimode fibre using an optical neural network chip
Zhengsen Ruan, Yuanjian Wan, Lulu Wang, Wei Zhou, Jian Wang
Published Published online: 12 July 2024 , doi: 10.37188/lam.2024.023

Mode-division multiplexing technology has been proposed as a crucial technique for enhancing communication capacity and alleviating growing communication demands. Optical switching, which is an essential component of optical communication systems, enables information exchange between channels. However, existing optical switching solutions are inadequate for addressing flexible information exchange among the mode channels. In this study, we introduced a flexible mode switching system in a multimode fibre based on an optical neural network chip. This system utilised the flexibility of on-chip optical neural networks along with an all-fibre orbital angular momentum (OAM) mode multiplexer-demultiplexer to achieve mode switching among the three OAM modes within a multimode fibre. The system adopted an improved gradient descent algorithm to achieve training for arbitrary 3 × 3 exchange matrices and ensured maximum crosstalk of less than −18.7 dB, thus enabling arbitrary inter-mode channel information exchange. The proposed optical-neural-network-based mode-switching system was experimentally validated by successfully transmitting different modulation formats across various modes. This innovative solution holds promise for providing effective optical switching in practical multimode communication networks.

Ultrafast laser processing of silk films by bulging and ablation for optical functional devices
Ming Qiao, Huimin Wang, Heng Guo, Ma Luo, Yuzhi Zhao, et al.
Published Published online: 12 July 2024 , doi: 10.37188/lam.2024.024

Organic proteins are attractive owing to their unique optical properties, remarkable mechanical characteristics, and biocompatibility. Manufacturing multifunctional structures on organic protein films is essential for practical applications; however, the controllable fabrication of specific structures remains challenging. Herein, we propose a strategy for creating specific structures on silk film surfaces by modulating the bulging and ablation of organic materials. Unique surface morphologies such as bulges and craters with continuously varying diameters were generated based on the controlled ultrafast laser-induced crystal-form transition and plasma ablation of the silk protein. Owing to the anisotropic optical properties of the bulge/crater structures with different periods, the fabricated organic films can be used for large-scale inkless color printing. By simultaneously engineering bulge/crater structures, we designed and demonstrated organic film-based optical functional devices that achieves holographic imaging and optical focusing. This study provides a promising strategy for the fabrication of multifunctional micro/nanostructures that can broaden the potential applications of organic materials.

Ultra-high-aspect-ratio structures through silicon using infrared laser pulses focused with axicon-lens doublets
Niladri Ganguly, Pol Sopeña, David Grojo
Published Published online: 10 July 2024 , doi: 10.37188/lam.2024.022

We describe how a direct combination of an axicon and a lens can represent a simple and efficient beam-shaping solution for laser material processing applications. We produce high-angle pseudo-Bessel micro-beams at 1550 nm, which would be difficult to produce by other methods. Combined with appropriate stretching of femtosecond pulses, we access optimized conditions inside semiconductors allowing us to develop high-aspect-ratio refractive-index writing methods. Using ultrafast microscopy techniques, we characterize the delivered local intensities and the triggered ionization dynamics inside silicon with 200-fs and 50-ps pulses. While similar plasma densities are produced in both cases, we show that repeated picosecond irradiation induces permanent modifications spontaneously growing shot-after-shot in the direction of the laser beam from front-surface damage to the back side of irradiated silicon wafers. The conditions for direct microexplosion and microchannel drilling similar to those today demonstrated for dielectrics still remain inaccessible. Nonetheless, this work evidences higher energy densities than those previously achieved in semiconductors and a novel percussion writing modality to create structures in silicon with aspect ratios exceeding ~700 without any motion of the beam. The estimated transient change of conductivity and measured ionization fronts at near luminal speed along the observed microplasma channels support the vision of vertical electrical connections optically controllable at GHz repetition rates. The permanent silicon modifications obtained by percussion writing are light-guiding structures according to a measured positive refractive index change exceeding 10−2. These findings open the door to unique monolithic solutions for electrical and optical through-silicon-vias which are key elements for vertical interconnections in 3D chip stacks.

Fine 3D control of THz emission in air with dual femtosecond laser pre-pulses at tunnelling ionisation regime
Hsin-Hui Huang, Takeshi Nagashima, Kota Kumagai, Yoshio Hayasaki, Saulius Juodkazis, et al.
Published Published online: 10 July 2024 , doi: 10.37188/lam.2024.030

Emission of THz radiation from air breakdown at focused ultra-short fs-laser pulses (800 nm/35 fs) was investigated for the 3D spatio-temporal control where two pre-pulses are used before the main-pulse. The laser pulse induced air breakdown forms a ~ 120 μm-long focal volume generate shockwaves which deliver a denser air into the focal region of the main pulse for enhanced generation of THz radiation at 0.1–2.5 THz spectral window. The intensity of pre- and main-pulses was at the tunnelling ionisation intensities (1–3) × 1016 W/cm2 and corresponded to sub-critical (transparent) plasma formation in air. Polarisation analysis of THz radiation revealed that orientation of the air density gradients generated by pre-pulses and their time-position locations defined the ellipticity of the generated THz electrical field. The rotational component of electric current is the origin of THz radiation.

A shoe-box-sized 3D laser nanoprinter based on two-step absorption
Tobias Messer, Michael Hippe, Jingya (Lilyn) Gao, Martin Wegener
Published Published online: 09 July 2024 , doi: 10.37188/lam.2024.027

State-of-the-art commercially available 3D laser micro- and nanoprinters using polymeric photoresists based on two- or multi-photon absorption rely on high-power pico- or femtosecond lasers, leading to fairly large and expensive instruments. Lately, we have introduced photoresists based on two-step absorption instead of two-photon absorption, allowing for the use of small and inexpensive continuous-wave 405 nm wavelength GaN semiconductor laser diodes with light-output powers below 1 mW. Here, using the identical photoresist system and similar laser diodes, we report on the design, construction, and characterization of a 3D laser nanoprinter that fits into a shoe box. This shoe box contains all optical components, namely the mounted laser, the collimation- and beam-shaping optics, a miniature MEMS xy-scanner, a tube lens, the focusing microscope objective lens (NA=1.4, 100× magnification), a piezo slip-stick z-stage, the sample holder, a camera monitoring system, LED sample illumination, as well as the miniaturized control electronics employing a microcontroller. We present a gallery of example 3D structures printed with this instrument. We achieve about 100 nm lateral spatial resolution and focus scan speeds of about 1 mm/s. Potentially, our shoe-box-sized system can be made orders of magnitude less expensive than today’ s commercial systems.

Parallel fabrication of silica optical microfibers and nanofibers
Hubiao Fang, Yu Xie, Zipei Yuan, Dawei Cai, Jianbin Zhang, et al.
Published Published online: 08 July 2024 , doi: 10.37188/lam.2024.020

Optical micro/nanofibers (MNFs) taper-drawn from silica fibers possess intriguing optical and mechanical properties. Recently, MNF array or MNFs with identical geometries have been attracting more and more attention, however, current fabrication technique can draw only one MNF at a time, with a low drawing speed (typically 0.1 mm/s) and a complicated process for high-precision control, making it inefficient in fabricating multiple MNFs. Here, we propose a parallel-fabrication approach to simultaneously drawing multiple (up to 20) MNFs with almost identical geometries. For fiber diameter larger than 500 nm, measured optical transmittances of all as-drawn MNFs exceed 96.7% at 1550-nm wavelength, with a diameter deviation within 5%. Our results pave a way towards high-yield fabrication of MNFs that may find applications from MNF-based optical sensors, optical manipulation to fiber-to-chip interconnection.

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